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Rheometer with in situ FTIR

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Rheometer

Contact details

Bose, Ranjita Dr.
Aerospace Engineering (LR), Novel Aerospace Materials
Kluyverweg 1, 2629HS Delft
Tel : +31 (0)15 27 82593
E-mail : r.k.bose@tudelft.nl
Website : Not available

General Information

Instrument:

Rheometer with in situ FTIR

Description

With a rheometer the steady state and time dependent viscoelastic properties of a material can be studied as a function of stress and/or strain. This equipment couples a rheometer with an in situ attenuated total reflectance Fourier transform infrared spectrometer (ATR-FTIR) which enables a simultaneous study of chemical information with rheological properties over a temperature range from ambient to 400 °C. Additionally, this equipment has a controlled test chamber with solid dynamic mechanical analysis (DMA) clamps for testing the viscoelastic properties of thin films from -150 °C to 600 °C.

Location:

Physical Lab, Aerospace Engineering

Key words:

rheology, viscoelastic properties, ATR FTIR, dynamic mechanical properties, elastic modulus, storage modulus

Instrument specification

Manufacturer: ThermoFisher

Model: Haake Mars III rheometer coupled with Nicolet iS10 FT-IR spectrometer

Torque 0.01 μNm to 200 mNm

Oscillation frequency 10-6 Hz to 100 Hz

Normal force 0.01 N to 50 N

Oven Temperature -150 °C to 600 °C

FTIR accessory temperature Ambient to 400 °C

FTIR range 400 to 4000 cm-1 wavenumber